50L New Type Glass Jacketed Reactor/ Double Layer Glass Reactor with Heating Bath

Basic Info

Model NO.	HEB-50L
Agitator Model	Anchor Agitator
Heating	Oil Circulation Heating
Heat Transfer Structure	Jacketed
Condition	New
Reactor Volume	50L
Interlayer Volume	About 16L
Stirring Speed	0-450rpm/Min
Vacuum	0.098MPa
Kettle Lid	Diameter 265mm 6 Ports
Overall Dimension(WDH)	8705602270mm
Net Weight	67kg
Transport Package	Wooden Box
Specification	HEB
Trademark	HEB
Origin	China
Production Capacity	1000sets

Product Description

50L New Type Glass Jacketed Reactor/ Double Layer Glass Reactor with Heating Bath

Circulation liquid of hot, cold or cryogenic can be filled into the jacket of reactor. Substance reacts by stirring under normal or negative pressure in aieproof glass container. Reaction process can be watched clearly through crystal reaction flask. Jacket Glass Reactor is ideal equipment in library experiment or medium-production in moden biology and pharmcy, and is also applied in synthesizing materials in fine chemical industry.

Working principle:

This machine has electric constant speed stirring system, condensation and dropping system. The interlayer of kettle body needs to be connected with heating or cooling circulation equipment. When the material is stirred, the circulating hot solution or cooling liquid is injected through the interlayer to make the materials in the kettle are heated or cooled at a constant temperature. When the material is heated and reacted, the evaporation efficiency can be improved under vacuum conditions (a vacuum device need to be connected). The solvent vapor is cooled into liquid when passing through the glass condensing coil (a cooling device need to be connected), which can be refluxed into the kettle. It can also be recycled through the lower valve of the dean-stark. When the reaction is completed, the material can be discharged from the side outlet at the bottom of the kettle.
This series of products need to be equipped with a vacuum device, a high-temperature or low-temperature circulation device to form system devices.

Basic configuration

• The parts in contact with the material are all made of high borosilicate glass (expansion coefficient 3.3) and PTFE materials, which have stable performance and are not easy to react with the materials.
• Using aluminum alloy + stainless steel material as frame body• Glass + PTFE discharge valve, side material discharge without effusion.• Low-speed power-increasing motor, electronic stepless speed regulation, fine adjustment by knob, speed control box with dual display function can digitally display the speed and the temperature of the material in the kettle.
• The stirring system adopts ceramic bearings and mechanical seals to prevent the stirring rod from wearing out.
• Using PT100 temperature sensor, 304 stainless steel material, wrapped by transparent PTFE tube outside , double anti-corrosion.
• Vacuum pressure gauge shows real-time vacuum by pointer.
• Crescent-type stirring paddle, 304 stainless steel + PTFE stirring blade; the material of the stirring rod is 304 stainless steel, and it is wrapped in PTFE tube outside.
• There is a universal wheel with brake at the bottom of the equipment, which can be moved as a whole and be operated conveniently.
• Fuse safety protection

Technical Parameters :

Model		HEB-50L
Reactor volume		50L, inner diameter 365mm, outer diameter 410mm, inner length 576mm
Interlayer volume		About 16L
Voltage/Frequency		220V 50HZ/110V 60Hz
Stirring motor power		120W1/3
Stirring speed		0-450rpm/min
Temperature range of reactor		-80ºC~+250ºC
Temperature measuring accuracy		±1ºC
Vacuum		0.098Mpa
Kettle lid Φ265mm 6 ports	Stirring port	Φ50mm flange port
	Condensing reflux port	50# ball mill port
	Port of constant pressure funnel	40# standard port
	Pressure relief port	34# standard port
	Temperature measuring port	Φ45mm flange port
	Solid feeding port	Φ80mm flange port, inner diameter Φ60mm, supporting PTFE cap
Stirring paddle		Φ17×1000H(mm) blade 190mm
Condenser		Φ100mm×700H(mm) lower Φ60mm flange port
Condensing area		0.4
Dean-stark		Upper Φ60 flange port, left 50# ball mill stopper
Constant pressure funnel		2L, upper 29# standard port with glass stopper; lower 40#standard stopper
Pressure relief valve		34# standard plug valve, releasing valve (pagoda joint) with 12mm outer diameter
Inlet and outlet circulation port of interlayer		Φ45mm flange port supporting flange plate, 1/2" male-PNT adapter
Material discharging port		Φ75mm flange, Φ33mm material discharging hole, oblique discharging valve(pagoda joint)Φ34mm, 350mm from the ground
Vacuum nozzle		Pagoda joint with 12mm outer diameter
In and out circulating nozzle of condenser coil		Pagoda joint with 15mm outer diameter
Overall dimension(WDH)		870×560×2270mm
Net weight		67KG
Packing dimension		1690×615×880mm wooden package 0.92m³
Packing weight		104KG